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 JACEN  Vol.6 No.1 , February 2017
Ethyl Levulinate Obtained from Lignocellulosic Waste Material with Previous Delignification by Ultrasonic-Assisted Technique
Abstract:
Ultrasound-assisted pretreatment under mild operating conditions has been investigated for intensification of delignification to facilitate the obtaining of ethyl levulinate from biomass. The effect of pH (2 - 12), temperature (30°C - 70°C) and pretreatment time (0 - 120 minutes) has been studied for different biomass samples. The most favorable conditions were basic pH, temperature of 70°C and pretreatment time of 2 h, obtaining values of delignification near 80 percent. The ethyl levulinate is obtained in microwave directly via from samples before and after delignification and analyzed for GC-MS. The results evidenced better yields for the delignified samples.
Cite this paper: Solá-Pérez, J. , Saldarriaga-Noreña, H. and Murillo-Tovar, M. (2017) Ethyl Levulinate Obtained from Lignocellulosic Waste Material with Previous Delignification by Ultrasonic-Assisted Technique. Journal of Agricultural Chemistry and Environment, 6, 93-103. doi: 10.4236/jacen.2017.61006.
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