ACES  Vol.1 No.1 , January 2011
Structural and Crystallographic Features of Chemically Synthesized Cero- and Titanium Cero- Antimonates Inorganic Ion Exchangers and Its Applications
ABSTRACT
Chemically synthesized cero-antimonate and titanium cero-antimonate prepared by sol-gel technique was conducted for the synthesis of a novel ion exchanger. The prepared materials has been characterized by X-ray diffraction, X-ray fluorescence, Fourier transform Infrared Spectroscopy (FT-IR) and Thermograve-metric analyses. The structures and empirical formula's was identified and found to CeSb4O12?6.19H2O and TiCeSb4O14?12.22H2O, for cero-antiomate and titanium cero-antimonate, respectively. The data obtained from X-ray diffraction was analyzed to define the crystallographic feature of cero-antimonate and titanium cero-antimonate and found both the composites were belong to cubic system with lattice constant 5.15 and 5.149 Å, respectively. The crystallite size and strain of cero-antimonate and titanium cero-antimonate were determined. By using ChemDraw Ultra program the modeling structures of cero-antimonate and titanium cero-antimonate were conducted. Finally, application of the prepared materials for the removal of heavy metals from industrial waste water in terms of capacity measurements was performed.

Cite this paper
nullM. Abou-Mesalam, "Structural and Crystallographic Features of Chemically Synthesized Cero- and Titanium Cero- Antimonates Inorganic Ion Exchangers and Its Applications," Advances in Chemical Engineering and Science, Vol. 1 No. 1, 2011, pp. 1-8. doi: 10.4236/aces.2011.11001.
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